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Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: 47

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
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table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

would read it as 20.18 mL.

Someone else might have a

slightly different estimation of

the last digit maybe they think

it is 20.16 mL or 20.19 mL.

This slight disagreement is fine

and gives an approximation of

the uncertainty of the

measurement. I would record

this value with four significant

digits since my last recorded

digit should be the one that

has uncertainty.

Buret readings should be

recorded to 2 decimal

places.

We determine the volume of

liquid delivered by reading the

volume at the beginning of the

titration and then reading the

volume again at the end of the

titration. The volume delivered

is then the difference between

those two readings:

Buret Preparation

We prep the buret by first rinsing with water multiple times and then rinsing

multiple times with the titrant solution we are using. To rinse the buret, we use

about 15 mL of liquid for each rinsing. Put the liquid into the buret with the

stopcock closed (perpendicular to the tip). Then slowly tilt the buret so that the

liquid touches all of the interior surface and finally allow the liquid to run out the

tip of the buret.

equation.pdf

47

Close-up of a buret showing meniscus and markings.

Figure 6.2: "Buret" by photobunny is licensed under CC BY-NC-ND 2.0. Figure 6.2: "Buret" by photobunny is licensed under CC BY-NC-ND 2.0.

Figure 6.2: "Buret" by photobunny is licensed under CC BY-NC-

ND 2.0.

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