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Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: Cleaning Glassware for Volumetric Measurements

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
Cleaning Glassware for Volumetric Measurements
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table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

Cleaning Glassware for Volumetric Measurements

Clean glassware is critical to achieving reliable results in the laboratory. For

volumetric measuring devices you are using, it is best to clean them with water

first and then to clean with the liquid that you will be using. The primary idea is

that a little bit of the liquid always gets left behind on surfaces, so the best thing

to do is ensure that the liquid left behind is the liquid you are using in the

measurement.

When rinsing glassware for cleaning, you should do multiple small volume

cleanings instead of one large volume cleaning. Rinsing a beaker three different

times with 10 mL of water each time is much more effective than rinsing once

with 30 mL of water. When rinsing make sure to coat all of the walls of the

glassware with the rinse liquid.

Volume Measuring Devices

Below are descriptions of some of the

common tools in the chemistry

laboratory for measuring volumes and

tips and tricks for using them.

Beakers and Erlenmeyer Flasks

Beakers and Erlenmeyer flasks are

convenient ways to work with liquids in

the laboratory because it is easy to add

and remove liquids to them. Beakers and

Erlenmeyer flasks come in many

different sizes (total volumes) and often

have markings along the side that

indicate additional volumes. For

example, a 100 mL beaker might have

markings every 10 mL and a main

marking at 100 mL.

It is tempting to use beakers and

Erlenmeyer flasks to measure a volume

because they are always readily

available, but the markings on these

tools are like the picture below, a “mL

inspired volume.”

24

Erlenmeyer flasks.

Figure 3.2: Erlenmeyer Flask: "Erlenmeyer Flasks 1" by biologycorner is licensed under CC BY-NC 2.0. Figure 3.2: Erlenmeyer Flask: "Erlenmeyer Flasks 1" by biologycorner is licensed under CC BY-NC 2.0.

Figure 3.2: Erlenmeyer Flask: "Erlenmeyer Flasks

1" by biologycorner is licensed under CC BY-NC

2.0.

Beaker with liquid

Figure 3.3: Beaker: "Siphon beaker" by niallkennedy is licensed under CC BY-NC 2.0. Figure 3.3: Beaker: "Siphon beaker" by niallkennedy is licensed under CC BY-NC 2.0.

Figure 3.3: Beaker: "Siphon beaker"

by niallkennedy is licensed under CC BY-NC 2.0.

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