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Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: 46

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
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table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

Titrations allow us to determine the number of moles of a compound in a sample.

Here is the key equation to understanding a titration where the coefficients refer

to the balanced chemical equation of the titrant reacting with the analyte:

Buret Introduction

For a titration to be quantitative, we need to determine how many moles of

titrant we have added. A buret is a commonly used piece of scientific equipment

to quantify the volume of liquid that has been delivered. We put a solution into

the buret that has a known molarity. We then determine the number of moles by

The buret has three main parts: 1. The tip of the buret is

where the liquid leaves the end of the buret, 2. The

stopcock is the valve near the tip of the buret that starts

and stops the flow of liquid from the buret, and 3. The neck

of the buret has volume markings that allow us to

determine how much liquid has left the buret.

When you are reading a buret, it is critical to make sure

that you take the time to look closely at the markings and

understand the spacing. In the picture in Figure 6.2 each

milliliter is marked (19, 20, 21, and 22). In addition, there

are nine lines in-between each milliliter value, so each of

these lines represents one-tenth of a milliliter. When

reading the buret in Figure 6.2, I see that the bottom of the

meniscus is in between the 1st and 2nd line after the 20 mL

mark. Notice that the bottom of the meniscus is likely to

not fall exactly on a marking which allows us to interpolate

the value to get the correct value along with an estimate of

the uncertainty.

My thought process for reading the buret is first to note

that the value is somewhere between 20 and 21 mL; then I

go a step further and see it is between 20.1 and 20.2 mL,

finally I determine the recorded value by estimating the last

digit. It looks as if it is closer to 20.2 mL than 20.1 mL so I

equation.pdf

equation.pdf

46

Buret used for titrations.

Figure 6.1: 50 mL buret. Figure 6.1: 50 mL buret.

Figure 6.1: 50 mL buret.

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