Skip to main content

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: 49

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
49
    • Notifications
    • Privacy
  • Project HomeNatural Sciences Collection: Anatomy, Biology, and Chemistry
  • Projects
  • Learn more about Manifold

Notes

Show the following:

  • Annotations
  • Resources
Search within:

Adjust appearance:

  • font
    Font style
  • color scheme
  • Margins
table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

titrant is added. Making sure that we are only adding one drop or less when the

solution changes color ensures that we are doing our best at finding the

equivalence point.

Common Errors to Avoid

Here are some common mistakes that you want to avoid when performing a

titration.

  1. Make sure the tip of your buret is fully filled with solution before starting the

titration. It is common for air bubbles to collect in the tip of the buret when

filling. If you don’t remove the air bubbles before beginning the titration, then

at some point the air bubble will run out of your buret and instead of

delivering 0.5 mL of solution, you will have delivered 0.5 mL of air.

  1. Remember the indicator. The titration only works if you can tell when the

equivalence point has been reached.

  1. Make sure to appropriately read the volume. Take the time to interpret the

markings on the buret and read the volume directly. Near the top of the buret

is marked 0 mL and near the bottom of the buret is marked 50 mL. Record the

current location of the bottom of the meniscus when reading.

  1. Avoid parallax errors when reading the buret. Parallax errors are avoided by

ensuring that your eye and the meniscus are at the same height when reading

the buret. This likely means you need to move either the location of your eye

or the location of the buret to appropriately take a reading. You can take the

buret out of the clamp to appropriately read the volume.

  1. Go slow at the end of the titration. Remember we want the solution to change

colors when we have only added a drop or less. 

49

Annotate

Next Chapter
50
PreviousNext
Lab Manuals
Powered by Manifold Scholarship. Learn more at
Opens in new tab or windowmanifoldapp.org