Skip to main content

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: 16

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
16
    • Notifications
    • Privacy
  • Project HomeNatural Sciences Collection: Anatomy, Biology, and Chemistry
  • Projects
  • Learn more about Manifold

Notes

Show the following:

  • Annotations
  • Resources
Search within:

Adjust appearance:

  • font
    Font style
  • color scheme
  • Margins
table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

In separating the mixture, we will use a few different techniques.

Heating with Bunsen Burner

Bunsen burners are effective ways to heat a sample. There are two adjustable

parameters on a Bunsen burner: the gas flow rate and the mixing ratio with air.

To ignite the Bunsen burner, first turn on the gas and then use a striker to ignite

the gas. Once the Bunsen burner is lit, the gas flow and mixing ratio are adjusted

to produce an efficient flame. An efficient flame has a sharp inner blue cone of

combustion.

If your Bunsen burner does not light, first check to make sure you have gas flow.

If you are properly turning on the gas and have flow, then check to see if the

striker is producing sparks when you use it. Test the striker a few times to make

sure you can consistently produce sparks. If you have gas flow and are producing

sparks, but the Bunsen burner still won’t light, then you need to adjust the air

mixing ratio. Turn the air mixing valve to minimize the amount of air that enters

the Bunsen burner. This should allow you to light the burner but then you will

need to increase the amount of air to produce a more intense flame.

Safety Considerations for a Bunsen Burner

Bunsen burners can pose serious risks in the laboratory. Probably one of the

most obvious risks is that you will use the Bunsen burner to heat objects, and

those hot objects can burn you if not handled appropriately. Remember that hot

glassware looks identical to cold glassware, so be aware of the temperature of a

laboratory tool before handling it.

You also risk igniting other objects. Make sure that paper and other flammable

materials are not near the Bunsen burner when lit. This is especially true for

flammable liquids. Make sure you are aware of the SDS requirements for the

materials you are using on a Bunsen burner. Flammable liquids should never be

used in the proximity of a Bunsen burner.

Aqueous Solubility (g/100 g water) at Various Temperatures

Substance

0 ºC

20 ºC

40 ºC

80 ºC

100 ºC

SiO2

0

0

0

0

0

NaCl

35.6

35.8

36.5

38.1

39.2

C6H5COOH

0.17

0.42

1.1

2.7

7.1

16

Annotate

Next Chapter
Experiment
PreviousNext
Lab Manuals
Powered by Manifold Scholarship. Learn more at
Opens in new tab or windowmanifoldapp.org