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Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: 53

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
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table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

Part Three

Determine the concentration of an H2SO4 solution via titration with 0.100 M

NaOH. Here H2SO4 is the analyte and NaOH is the titrant. Each laboratory partner

should successfully complete one titration of the H2SO4 solution following the

general steps on the previous page. Use a 10.00 mL volumetric pipet to add the

analyte to the Erlenmeyer flask. Add additional water to the flask to bring the

total volume to somewhere between 25 and 50 mL. Check that your laboratory

partner does the following when completing their titration:

•Is analyte added to flask with volumetric pipet?

•Is the indicator added to the flask?

•Is the initial volume of buret recorded to 2 decimal places?

•Does the solution turn color with the addition of one drop or less of

titrant solution?

•Is final volume of buret recorded to 2 decimal places?

•Is waste solution appropriately disposed of?

Sample Data Table for Part Three

•Volume of H2SO4 Added to Flask (mL):

•Molarity of NaOH (M):

•Initial Volume Reading of Buret (mL):

•Final Volume Reading of Buret (mL):

•Volume Added (mL):

•Moles of NaOH Added (moles):

•Moles of H2SO4 in Flask (moles):

•Molarity of H2SO4 (M):

53

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