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Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: 29

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
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table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

  1. Take the pipet out of the liquid and wipe off the outside of the pipet.
  1. Place the tip of the pipet into a new container, release the pressure from your

finger, and allow the liquid to flow down the wall of the container.

  1. You will notice that there is a small amount of liquid remaining in the tip of

the pipet. Leave that small amount of liquid in the pipet. The small amount of

liquid is supposed to be there as the pipets

are designed as TD (to deliver) pipets and

calibrated knowing that the small amount

of liquid gets left behind.

Volumetric Flasks

Volumetric pipets are designed to deliver a

specific volume, whereas volumetric flasks

are designed to contain a specific volume.

Like volumetric pipets, volumetric flasks are

designed for only one specific volume, so if

you want a different volume, then you need

to use a different volumetric flask.

When filling a volumetric flask, you need to

be careful when the liquid approaches the

line because you will need to start completely

over once it passes the line. It is helpful to

use a dropper to control the last bit of liquid

added to ensure that it is not filled above the

line.

29

Volumetric flask.

Figure 3.9: Volumetric Flask: "File:Brand volumetric flask 100ml.jpg" by Lucasbosch is licensed under CC BY-SA 3.0. Figure 3.9: Volumetric Flask: "File:Brand volumetric flask 100ml.jpg" by Lucasbosch is licensed under CC BY-SA 3.0.

Figure 3.9: Volumetric Flask: "File:Brand

volumetric flask 100ml.jpg"

by Lucasbosch is licensed under CC BY-SA

3.0.

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Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
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