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Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual: Laboratory Notebook

Chemistry Techniques and Explorations: An Introductory Chemistry Laboratory Manual
Laboratory Notebook
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table of contents
  1. About PA-ADOPT
  2. About OER
  3. About the Author
    1. Author Acknowledgements
    2. Goal of Laboratory Manual
  4. Table of Contents
  5. Safety and Record Keeping
    1. Safety Rules
    2. RAMP Approach to Safety
    3. Laboratory Notebook
    4. References
  6. Separating Substances, Measuring Mass, and Analyzing Data - Technique Laboratory
    1. Introduction for Measurement of Masses
    2. Separating a Heterogeneous Mixture and Determining Masses
    3. Experiment
    4. Safety Considerations
    5. Waste Disposal
    6. Introduction for Treatment of Data
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  7. Measuring Volumes - Technique Laboratory
    1. Motivation
    2. Cleaning Glassware for Volumetric Measurements
    3. Volume Measuring Devices
    4. Practice Technique for Graduated Cylinder, Volumetric Pipet, and Volumetric Flask
    5. Waste Disposal
    6. Safety Considerations
    7. Pre-Lab Questions
    8. Post-Lab Calculations and Questions
  8. Reaction Types and Qualitative Analysis - Technique Laboratory
    1. Introduction
    2. Observing Chemical Reactions
    3. Oxidation-Reduction Reactions: Movement of electrons
    4. Acid-Base Reactions: Movement of H+
    5. Precipitation Reactions: Solid Formation
    6. Flame Tests
    7. Safety Considerations
    8. Waste Disposal
    9. Pre-lab Questions
    10. Post-Lab Questions
  9. What is Contaminating the Water Supply? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Available Materials
    4. Data Collection
    5. Safety Considerations
    6. Waste Disposal
    7. Pre-Lab Questions
    8. Post-Lab Questions
  10. Titrations Technique Laboratory
    1. Titration Background and Application
    2. Safety Considerations
    3. Disposal of Waste
    4. Laboratory Activities
    5. Calculations
    6. Pre-Lab Questions
    7. Post-Lab Questions
    8. References
  11. What is the Acidity of Vinegar? - Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References
  12. Absorption Spectroscopy Technique Laboratory
    1. Absorbance Spectroscopy Background
    2. Ultraviolet-Visible Absorbance Spectroscopy
    3. Safety Considerations
    4. Disposal of Waste
    5. Laboratory Activities
    6. Calculations
    7. Pre-Lab Questions
    8. Post-Lab Questions
    9. References
  13. What is the Dye Composition of a Drink?-Exploration Laboratory
    1. Background
    2. Experiment
    3. Safety Considerations
    4. Disposal of Waste
    5. Pre-Lab Questions
    6. Post-Lab Questions
    7. References

Laboratory Notebook

The laboratory notebook is where all information about laboratory experiments

should be stored. The idea is that the laboratory notebook is a permanent record

of all preparation, all observations and data in the laboratory, and all analysis of

data after an experiment. The main purpose is to record all that you have done

so that you and others can look at the notebook and replicate experiments.

Laboratory notebooks are routinely used in court cases to determine if samples

were handled properly and who gets awarded patents for new technology.

Guidelines for Maintaining a Laboratory Notebook

•Table of Contents is kept current with page numbers.

•Pages are numbered consecutively and no blank spaces are left in the

notebook.

•All entries are made in permanent ink at the time of the observation.

•Errors are corrected by crossing out with a single line, initialing the

correction, and dating when the correction was made.

•Procedures for the experiments are well documented.

•Notebook is signed and dated to document when data entry begins and

ends.

•Data and observations are recorded in an organized fashion.

•Data are recorded with appropriate units and significant figures.

•Notebook is signed by a witness at the end of data collection.

•Sample calculations and details of data analysis are provided.

•Summary of findings is recorded after the experiment.

References

American Chemical Society, “Guidelines for Chemical Laboratory Safety in

Academic Institutions.” 2016, https://www.acs.org/content/dam/acsorg/about/

governance/committees/chemicalsafety/publications/acs-safety-guidelines-

academic.pdf Accessed: February 26, 2023.

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